反应详情

To a solution of 4,4-dimethylcyclohexanone (0.511 g, 4.049 mmol) in 95% ethanol (20 ml) was added 50% hydroxylamine in water (2.481 ml, 40.49 mmol), and the reaction was heated to reflux for 2 hours. The reaction was cooled to ambient temperature, and the product was precipitated by the addition of water. The solids were collected by vacuum filtration to yield 202 mg of the title compound (35% yield).

1. temperaturethe reaction was heated
2. temperatureto reflux for 2 hours
3. customthe product was precipitated by the addition of water
4. filtrationThe solids were collected by vacuum filtration