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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 510972Generated: October 30, 2026

HCID 123212539, compound → HCID 86666884, compound

https://huagongshe.com/reaction/510972

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 123212539HCID 123212539—
SolventHydrochloric AcidHCID 313—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 86666884HCID 86666884—

Reaction Steps

The tert-butyl [1-(5-chloro-3-{6-[(dimethylamino)carbonyl]pyridin-2-yl}-2-methoxy-4-methylphenyl)ethyl]carbamate (0.06 gm, 0.13 mmol) was dissolved in 4 M HCl in dioxane (3 mL) and was stirred for 1 hour. The reaction was complete and the mixture was concentrated in vacuo to give the crude product as an oil. LCMS calculated for C18H23ClN3O2(M+H)+: m/z=348.1. found: 348.1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09096600B2
Source datasetuspto-grants-2015_08
ORD IDord-a23dabb60f934940bd8bbd09dbcc0cf2
Source noteuspto-grants-2015_08