HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66798230, compound → HCID 66798061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66798230 | HCID 66798230 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 66798061 | HCID 66798061 | — |
Reaction Steps
7-(4-Hydroxybut-1-ynyl)-9,10-dihydrophenanthren-2-ol is dissolved in THF and hydrogenated to completion on palladium/active carbon catalyst. The catalyst is filtered off, the solvent is removed in vacuo, and the residue is recrystallised from toluene, giving 7-(4-hydroxybutyl)-9,10-dihydrophenanthren-2-ol as colourless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096795B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-972c8aba42c74e89b73e9da14e1c0e56 |
| Source note | uspto-grants-2015_08 |