HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl fluorosulfate → 3-(4-Methoxybenzylthio)-1-methylquinuclidinium fluorosulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl fluorosulfate | HCID 9870 | — |
| Reactant | 3-(4-Methoxybenzylthio)quinuclidine | HCID 19797265 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3-(4-Methoxybenzylthio)-1-methylquinuclidinium fluorosulfonate | HCID 19797250 | — |
Reaction Steps
The procedure described in Preparation 6-(3) was repeated, but using 756 mg of 3-(4-methoxybenzylthio)-quinuclidine and 271 μl of methyl fluorosulfonate in the presence of 5 ml of methylene chloride, to afford 1.078 g of the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05242914 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-2f5f24183fd544bba8168c7d1c51e356 |
| Source note | uspto-grants-1993_09 |