HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Chloromethyl)-2-fluoro-5-methoxy-4-nitrobenzene → 5-(Chloromethyl)-1-fluoro-3-methoxy-2-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Chloromethyl)-2-fluoro-5-methoxy-4-nitrobenzene | HCID 67255107 | — |
| Reactant | (3-Fluoro-5-methoxy-4-nitrophenyl)methanol | HCID 67256643 | — |
| Product | 5-(Chloromethyl)-1-fluoro-3-methoxy-2-nitrobenzene | HCID 67254475 | — |
Reaction Steps
The title compound was prepared using the procedure from Compound 130C (1-(chloromethyl)-2-fluoro-5-methoxy-4-nitrobenzene) with (3-fluoro-5-methoxy-4-nitrophenyl)methanol (Compound 146D). 1H NMR (CDCl3, 400 MHz): δ=3.96 (s, 3 H), 4.55 (s, 2 H), 6.87-6.90 (m, 2 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096624B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-0e4044d231d1425090ccc8df184f2fea |
| Source note | uspto-grants-2015_08 |