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HRID511357

反应详情

EQUATION

反应方程式

HRID 511357 的结构方程式

REACTANTS

反应物

2
结构：COc1c([N+](=O)[O-])ccc(CCl)c1F
HCID67254948

Benzene, 1-(chloromethyl)-2-fluoro-3-methoxy-4-nitro-

C8H7ClFNO3

2 次

结构：CCOP(=O)(Cc1ccc([N+](=O)[O-])c(Cl)c1)OCC
HCID86654007

Phosphonic acid, P-[(3-chloro-4-nitrophenyl)methyl]-, diethyl ester

C11H15ClNO5P

PRODUCTS

生成物

1
结构：CCOP(=O)(Cc1ccc([N+](=O)[O-])c(OC)c1F)OCC
HCID86654025

未命名化合物

PROCEDURE

实验过程

The title compound was prepared using the procedure from Compound 104C (Diethyl (3-chloro-4-nitrobenzyl)phosphonate) with 1-(chloromethyl)-2-fluoro-3-methoxy-4-nitrobenzene (Compound 147C). 1H NMR (CDCl3, 400 MHz): δ=1.28-1.32 (m, 6 H), 3.19-3.31 (m, 2 H), 7.14-7.22 (m, 1 H), 7.54-7.61 (m, 1 H). MS (ES+): m/z 322.08 [MH+] (TOF, polar).