HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-3-methoxy-4-nitrobenzoic acid → (2-Fluoro-3-methoxy-4-nitrophenyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-3-methoxy-4-nitrobenzoic acid | HCID 57955623 | — |
| Reactant | (2-Fluoro-5-methoxy-4-nitrophenyl)methanol | HCID 67255286 | — |
| Product | (2-Fluoro-3-methoxy-4-nitrophenyl)methanol | HCID 67254223 | — |
Reaction Steps
The title compound was prepared using the procedure from Compound 130D ((2-fluoro-5-methoxy-4-nitrophenyl)methanol) with 2-fluoro-3-methoxy-4-nitrobenzoic acid (Compound 147E). 1H NMR (CDCl3, 400 MHz): δ=4.08 (d, J=1.77 Hz, 3 H), 4.85 (s, 2 H), 7.29-7.35 (m, 1 H), 7.64 (dd, J=8.46, 1.89 Hz, 1 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096624B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-edea00627a624e24a8a9bc4b74a5b216 |
| Source note | uspto-grants-2015_08 |