HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Formaldehyde bis(4-n-butylcyclohexylthio)acetal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 22737665 | HCID 22737665 | — |
| Product | Formaldehyde bis(4-n-butylcyclohexylthio)acetal | HCID 22737691 | 107.4% |
Reaction Steps
Synthesis was conducted as in Synthesis Example 2 using 44.6 g (0.23 mol) of the 4-n-butylcyclohexylmercaptan prepared above, 10.7 g (0.26 mol) of sodium hydroxide, 92 g of ethanol and 16.1 g (0.19 mol) of dichloromethane. There was obtained 48.0 g of the desired formaldehyde bis(4-n-butylcyclohexylthio)acetal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06713612B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-cefca4276fa245e19c1b3174ec5411a2 |
| Source note | uspto-grants-2004_03 |