HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 22737626, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-Propylcyclohexane-1-thiol | HCID 22737660 | — |
| Product | HCID 22737626 | HCID 22737626 | 103.9% |
Reaction Steps
Synthesis was conducted as in Synthesis Example 2 using 38.1 g (0.22 mol) of the 4-n-propylcyclohexylmercaptan prepared above, 9.4 g (0.23 mol) of sodium hydroxide, 77 g of ethanol and 14.3 g (0.17 mol) of dichloromethane. There was obtained 41.2 g of the desired formaldehyde bis(4-n-propylcyclohexylthio)acetal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06713612B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-5c52de48c65d4f0fa85cd406f282a05a |
| Source note | uspto-grants-2004_03 |