HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86675010, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 67209003 | HCID 67209003 | — |
| Catalyst | Pyridine | HCID 1049 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86675010 | HCID 86675010 | 106.8% |
Reaction Steps
5 g (22 mmol) of 2-(isopropoxycarbonyloxy)benzoic acid are dissolved in 50 ml of dichloromethane with a few drops of pyridine. 1.95 ml (27 mmol) of thionyl chloride are added dropwise and the mixture is stirred at ambient temperature for 18 h and then concentrated to dryness. 5.7 g of 2-(isopropoxycarbonyloxy)benzoyl chloride are obtained with a quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102607B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-aeef175910b24d7692b17f71965d9d91 |
| Source note | uspto-grants-2015_08 |