HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 66930869, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 66931163 | HCID 66931163 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66930869 | HCID 66930869 | — |
Reaction Steps
7-Bromo-1-(2-hydroxy-phenyl)-heptane (9.3) was synthesized as in 9.1 using 8.3 (0.30 g, 1.01 mmol) in anhydrous CH2Cl2 (10 mL), and BBr3 (1M solution in CH2Cl2, 2.2 mL, 2.2 mmol). The title compound (9.3) was isolated as a viscous liquid after purification by flash column chromatography (0.247 g, 90% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102622B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-eb64d0b098fe413babe51c74fbbdbdc3 |
| Source note | uspto-grants-2015_08 |