HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride etherate → HCID 23725185, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | HCID 25017346 | HCID 25017346 | — |
| Solvent | 1,1-Ethanedithiol | HCID 33645 | — |
| Product | HCID 23725185 | HCID 23725185 | 70.8% |
Reaction Steps
7-(2-Hydroxy-phenyl)-heptanesulfonyl fluoride (14.3) was synthesized as described in 14.1 using 13.3 (0.065 g, 0.17 mmol) in ethanedithiol (5 mL) and BF3.Et2O (0.092 g, 0.65 mmol). Purification by flash column chromatography gave 14.3 (0.033 g, 70% yield) as a viscous liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102622B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-bf41d6e3025a42889c28941f381fa978 |
| Source note | uspto-grants-2015_08 |