HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxybenzaldehyde → HCID 57999445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxybenzaldehyde | HCID 11569 | — |
| Reactant | HCID 20213174 | HCID 20213174 | — |
| Reactant | HCID 57999483 | HCID 57999483 | — |
| Product | HCID 57999445 | HCID 57999445 | 53.4% |
Reaction Steps
The synthesis was carried out analogous to the preparation of 77 using 79 (0.14 g, 1.03 mmol) and 63 (0.29 g, 3.45 mmol). Purification by flash column chromatography on silica gel gave compound 80 (0.12 g, 53.4% yield) as a viscous liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102622B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-59f3b3b1bd3b4b45b531443ffc6d761e |
| Source note | uspto-grants-2015_08 |