2-Chlorobenzoic Acid → HCID 86716428, compound

HRID 512373Notes

Reaction equation

HRID 512373 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH:11]1([CH2:14][CH:15]([C:18]2[CH:23]=[N:22][C:21]([CH3:24])=[CH:20][N:19]=2)[CH2:16][NH2:17])[CH2:13][CH2:12]1>>[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH:17][CH2:16][CH:15]([C:18]1[CH:23]=[N:22][C:21]([CH3:24])=[CH:20][N:19]=1)[CH2:14][CH:11]1[CH2:13][CH2:12]1)=[O:6]

Participants

3

Reactant 2

HCID 83742-Chlorobenzoic AcidHCID 86716429HCID 86716429, compound

Product 1

HCID 86716428HCID 86716428, compound

Procedure

From 2-chlorobenzoic acid and 3-cyclopropyl-2-(5-methylpyrazin-2-yl)propylamine. LCMS (MH+): m/z=330.0, tR (minutes, Method E)=0.61

Sources & evidence

ORD record
ord-86a6b576f88d4078ab318248a5f3fbbc
Source dataset
uspto-grants-2015_08
Patent number
US09102591B2

Reaction notes

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