2,3-Dichlorobenzoic acid → HCID 86716340, compound

Participants

Reaction Steps

The racemic mixture which was prepared in a similar manner to example 3a from 2,3-dichlorobenzoic acid and 2-(5-(1-amino-3-cyclopropylpropan-2-yl)pyridin-2-yl)propan-2-ol was separated into the two enantiomers by preparative SFC to yield the title compound. LCMS (MH+): m/z=407.1, tR (minutes, Method F)=1.98. [α]D20=+23.89 (c=3.0 mg/mL,CHCl3)

Provenance & Evidence