HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 22113416, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 22113414 | HCID 22113414 | — |
| Product | HCID 22113416 | HCID 22113416 | — |
Reaction Steps
11.0 g (49.4 mmol) of 6-[chloro(difluoro)methyl]-2-oxo-1,2-dihydropyridine-3-carboxamide were heated in 77 ml of 50% strength sulfuric acid. The mixture was then added to ice water, and the precipitate was filtered off with suction and dried. This gave 7.2 g (65% of theory) of a yellowish powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102623B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-f78862d54f8345d0b9488d62062b1807 |
| Source note | uspto-grants-2015_08 |