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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 512536Generated: November 1, 2026

Potassium Carbonate → HCID 72550412, compound

https://huagongshe.com/reaction/512536

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 86703374HCID 86703374—
CatalystWaterHCID 962—
SolventMethanolHCID 887—
ProductHCID 72550412HCID 725504128.7%

Reaction Steps

To a mixture of 5-[4-(2-acetoxyacetamido)benzamido]-2-(naphthalen-2-ylamino)thiazole-4-carboxamide (0.10 g, 0.20 mmol) in MeOH (10 mL) was added K2CO3 (0.14 g, 0.99 mmol) and 1 drop of water at rt. The mixture was stirred for 16 hrs at rt. The insoluble material was filtered off, and the filtrate was concentrated in vacuo. The resulting solids were collected and washed with Et2O to give 0.008 g (5% yield) of the titled compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09102637B2
Source datasetuspto-grants-2015_08
ORD IDord-9faac0b603f9427c8fb880cca8774b66
Source noteuspto-grants-2015_08