HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 72550412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 86703374 | HCID 86703374 | — |
| Catalyst | Water | HCID 962 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 72550412 | HCID 72550412 | 8.7% |
Reaction Steps
To a mixture of 5-[4-(2-acetoxyacetamido)benzamido]-2-(naphthalen-2-ylamino)thiazole-4-carboxamide (0.10 g, 0.20 mmol) in MeOH (10 mL) was added K2CO3 (0.14 g, 0.99 mmol) and 1 drop of water at rt. The mixture was stirred for 16 hrs at rt. The insoluble material was filtered off, and the filtrate was concentrated in vacuo. The resulting solids were collected and washed with Et2O to give 0.008 g (5% yield) of the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102637B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-9faac0b603f9427c8fb880cca8774b66 |
| Source note | uspto-grants-2015_08 |