HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycerol → 74525-47-6
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycerol | HCID 753 | — |
| Reactant | Sodium 3-nitrobenzenesulfonate | HCID 31389 | — |
| Reactant | 3-Isopropylaniline | HCID 458679 | — |
| Product | 74525-47-6 | HCID 20562897 | 102.6% |
Reaction Steps
In a similar fashion using route 10 general procedure 20, 3-isopropylaniline (1 g, 7.4 mmol), glycerol (2.11 g, 22.9 mmol) and 3-nitro benzenesulfonic acid sodium salt (2.2 g, 9.61 mmol) gave the title compound (1.3 g, 100%) which was used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-d7a25d8ba2ae454d86500fa212560981 |
| Source note | uspto-grants-2015_08 |