HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 12363388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 7-Ethylquinoline | HCID 24311 | — |
| Reactant | Potassium Nitrate | HCID 24434 | — |
| Product | HCID 12363388 | HCID 12363388 | 12% |
Reaction Steps
In a similar fashion using route 7 general procedure 15, 7-ethylquinoline (Intermediate 57) (1.21 g, 7.7 mmol), potassium nitrate (1.01 g, 10.0 mmol) and H2SO4 (3.6 ml) gave the title compound (170 mg, 12%) after purification by column chromatography with n-hexane/EtOAc (23:2-17:3) gradient elution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-fa312705a4f942b289e5c8d665c0b0d8 |
| Source note | uspto-grants-2015_08 |