HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 12215944, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Sulfite | HCID 24437 | — |
| Reactant | 2-Fluoro-1-methyl-3-nitrobenzene | HCID 13470957 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12215944 | HCID 12215944 | 205.9% |
Reaction Steps
In a similar fashion using route 39 general procedure 95, 2-fluoro-3-nitrotoluene (2.5 g 16.1 mmol) in EtOH (60 ml) and Na2SO3 (4.61 g, 36.58 mmol) in EtOH: water (40 ml: 50 ml) at 70° C. for 16 h gave the title compound (7.2 g) which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-b20dda2443e64d87861e0f6801417fcd |
| Source note | uspto-grants-2015_08 |