HRID513759

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID222

Ammonia gas

H3N

结构：O=S1(=O)Nc2c(ccc3c(Cl)ccnc23)-c2ccccc21

HCID68183355

未命名化合物

PRODUCTS

生成物

结构：Nc1ccnc2c3c(ccc12)-c1ccccc1S(=O)(=O)N3

HCID68190282

未命名化合物

收率 20%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

In a similar fashion using route 48 general procedure 114, 1-chloro-5H-6-thia-4,5-diaza-chrysene 6,6-dioxide 305 (90 mg, 0.28 mmol), 7M NH3 in MeOH (5 ml) gave the title compound (17 mg, 20%) after purification by column chromatography eluting with chloroform/MeOH (98:2:1 drop NH3).