Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 513761Generated: October 31, 2026

Hydrochloric Acid → HCID 68183405, compound

https://huagongshe.com/reaction/513761

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantEthanolHCID 702—
ReactantStannous ChlorideHCID 24479—
ReactantHCID 86669769HCID 86669769—
ProductHCID 68183405HCID 6818340574%

Reaction Steps

In a similar fashion using route 2 general procedure 4,4-dimethylamino-2-nitro-N-quinolin-8-yl-benzenesulfonamide 500 (140 mg, 0.37 mmol), SnCl2 (210 mg, 1.12 mmol), 6N HCl (1 ml) and EtOH (5 ml) at 80° C. for 6 h gave the title compound (95 mg, 74%) which was used in the next step without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09102688B2
Source datasetuspto-grants-2015_08
ORD IDord-780d6933f3904cf4b137172dbec4c2c2
Source noteuspto-grants-2015_08