HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68190293, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 131733284 | HCID 131733284 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68190293 | HCID 68190293 | 73.4% |
Reaction Steps
In a similar fashion using route 55 general procedure 124, 12-chloro-6,6-dioxo-5,6-dihydro-6λ*6*-thia-4,5-diaza-chrysene-9-carboxylic acid 1-tert-butoxycarbonyl-pyrrolidin-3-yl ester (70 mg, 0.13 mmol) and 4M HCl in dioxane (3 ml) gave the title compound (41 mg, 73%) after washing with MeOH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-dcd207e86b1c40479f4c583568df11dc |
| Source note | uspto-grants-2015_08 |