HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfamide → HCID 68183113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfamide | HCID 82267 | — |
| Reactant | HCID 131733286 | HCID 131733286 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 68183113 | HCID 68183113 | 12.7% |
Reaction Steps
In a similar fashion using route 63 general procedure 140, N*7*-(4-trifluoromethyl-benzyl)-quinoline-7,8-diamine 577 (334 mg, 1.0 mmol), sulfamide (154 mg, 1.5 mmol) and pyridine (5 ml) gave the title compound (48 mg, 12%) after purification by preparative HPLC (acidic conditions 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-f7a0d1b8fe3349fabf242ee7137af458 |
| Source note | uspto-grants-2015_08 |