HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2,4-Dichlorophenyl)-3-methylnaphthalen-2-ol → 1-(2,4-Dichlorophenyl)-3-methylnaphthalen-2-yl trifluoromethanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2,4-Dichlorophenyl)-3-methylnaphthalen-2-ol | HCID 67126134 | — |
| Reactant | 1-Chloro-3-methylnaphthalen-2-yl trifluoromethanesulfonate | HCID 86691531 | — |
| Product | 1-(2,4-Dichlorophenyl)-3-methylnaphthalen-2-yl trifluoromethanesulfonate | HCID 86691537 | — |
Reaction Steps
1-(2,4-dichlorophenyl)-3-methylnaphthalen-2-yl trifluoromethanesulfonate was prepared in a similar manner as compound 4C in Example 2, except starting from 1-(2,4-dichlorophenyl)-3-methylnaphthalen-2-ol instead of 4B. 1H-NMR: 400 MHz, (CDCl3) δ: 7.85-7.90 (m, 2H), 7.62 (d, 1H), 7.55 (app dt, 1H), 7.41-7.48 (m, 2H), 7.32-7.49 (m, 2H), 2.64 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102614B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-81e47063a1d647bfa293406bc2e462d5 |
| Source note | uspto-grants-2015_08 |