Ethylamine → HCID 68292791, compound

Participants

Reaction Steps

2.17 g (8.40 mmol) of 2-chloro-N-cyclopropyl-4-fluoro-5-nitrobenzamide were initially charged in 100 ml of THF, 12 ml of a 2 molar solution of ethylamine in THF (16.79 mmol) were added and the mixture was stirred in a closed ampoule at room temperature for 18 hours. The reaction mixture was poured onto water, the organic solvents were distilled off and the residue obtained was filtered off with suction. Yield: 2.10 g (81% of theory)

Provenance & Evidence