HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 58258503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 58258448 | HCID 58258448 | — |
| Product | HCID 58258503 | HCID 58258503 | — |
Reaction Steps
A mixture of pyrrolidine (150 ml) and water (15 ml) was stirred at r.t. 1-[[3-chloro-4-(2,2-dibromoethenyl)phenyl]methyl]-pyrrolidine (crude, max. 44.70 mmol) was added to the mixture and subsequently, the mixture was stirred overnight at r.t. The solvent was evaporated, yielding 1-[[2-chloro-4-(1-pyrrolidinylmethyl)phenyl]acetyl]-pyrrolidine as a crude that was used as such in the next reaction step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09107946B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-d4ace16a01b54ee0806cc9dc163f3e3c |
| Source note | uspto-grants-2015_08 |