HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium tert-butoxide → HCID 56971610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Reactant | HCID 86693811 | HCID 86693811 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 56971610 | HCID 56971610 | — |
Reaction Steps
To a solution of ethyl N-benzyloxycarbonyl-N-{(2-cyclopropylaminocarbonyl)ethyl}aminoacetate (200 mg, 0.574 mmol) in toluene (2.0 mL) was added potassium tert-butoxide (136 mg, 1.21 mmol) as a base at an outer temperature set of 40° C., followed by stirring for 2 hours. Then, the HPLC measurement of this reaction mixture was carried out. The results are shown in Table 5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09108915B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-7bbb4c8df3694d58a909f46abaf55a9d |
| Source note | uspto-grants-2015_08 |