HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Benzyl-5-phenyl-1,4-oxazepane → 5-Phenyl-1,4-oxazepane hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Benzyl-5-phenyl-1,4-oxazepane | HCID 66718543 | — |
| Reactant | 5-Methyl-1,4-oxazepane hydrochloride | HCID 66718639 | — |
| Product | 5-Phenyl-1,4-oxazepane hydrochloride | HCID 66718510 | — |
Reaction Steps
5-Phenyl-[1,4]oxazepane hydrochloride was prepared by the same procedure as that of 5-methyl-[1,4]oxazepane hydrochloride except for utilizing 4-benzyl-5-phenyl-[1,4]oxazepane instead of 4-benzyl-5-methyl-[1,4]oxazepane. Then 5-phenyl-[1,4]oxazepane hydrochloride was obtained as white solid (0.14 g, 0.65 mmol, 73%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09108957B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-c80cd0e3a3274aaf81da6b56f42ac077 |
| Source note | uspto-grants-2015_08 |