HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → Benzeneacetic acid, 3,5-dichloro-, methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 1196155-85-7 | HCID 72211296 | — |
| Product | Benzeneacetic acid, 3,5-dichloro-, methyl ester | HCID 67195643 | 91% |
Reaction Steps
To methyl 3,5-dichlorobenzeneethanimidate hydrochloride (1:1) (i.e. the product from Step A1a) (50 g, 0.107 mol) was added to a mixture of toluene (167 mL) and water (167 mL). After 60 min the organic phase was removed, dried (MgSO4), and evaporated to give the title compound as an oil (39 g, 91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09108965B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-e6b80a59adf2446fb06a3f78c2275abc |
| Source note | uspto-grants-2015_08 |