HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131733308, compound → HCID 29946850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131733308 | HCID 131733308 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 29946850 | HCID 29946850 | — |
Reaction Steps
To a solution of 21 g (53 mmol) of the compound obtained in Step D in 600 mL of ethyl acetate there are added 2.1 g of palladium-on-carbon 10%. The batch is stirred at ambient temperature under a pressure of 1.3 bars of dihydrogen for 5 hours. The reaction mixture is then filtered and then concentrated to dryness. The title product is obtained in the form of a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09108983B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-473aa7073d114a5bb58a04d668086f8b |
| Source note | uspto-grants-2015_08 |