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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 515884Generated: October 30, 2026

HCID 131733308, compound → HCID 29946850, compound

https://huagongshe.com/reaction/515884

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 131733308HCID 131733308—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 29946850HCID 29946850—

Reaction Steps

To a solution of 21 g (53 mmol) of the compound obtained in Step D in 600 mL of ethyl acetate there are added 2.1 g of palladium-on-carbon 10%. The batch is stirred at ambient temperature under a pressure of 1.3 bars of dihydrogen for 5 hours. The reaction mixture is then filtered and then concentrated to dryness. The title product is obtained in the form of a solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09108983B2
Source datasetuspto-grants-2015_08
ORD IDord-473aa7073d114a5bb58a04d668086f8b
Source noteuspto-grants-2015_08