HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 117831357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 131733310 | HCID 131733310 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 117831357 | HCID 117831357 | — |
Reaction Steps
To a solution of 9.5 g (17.97 mmol) of the compound obtained in Step B in 40 mL of dioxane there are added, dropwise, 20 mL of a 4M solution of HCl in dioxane. The batch is stirred at ambient temperature for 48 hours and then the solution is concentrated to dryness. After drying, the expected product is obtained in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09108983B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-1b3c743a63b747fca9a93b840acaaa52 |
| Source note | uspto-grants-2015_08 |