HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178525525, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178519222 | HCID 178519222 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 178525525 | HCID 178525525 | 102.2% |
Reaction Steps
A 1 M NaOH (0.3 ml, 0.30 mmol) was added to a solution of 3-cyclopentyl-4-(cis-4-hydroxycyclohexyl)furan-2,5-dione (40 mg, 0.15 mmol) in 1,4-dioxane (1.0 ml) at room temperature, and the mixture was stirred for 3 hr. The reaction mixture was concentrated, and the residue was dried in vacuo to give the title compound as a colorless solid (50 mg, quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09115079B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-6d2038cc89c2486d886415f0edf766e0 |
| Source note | uspto-grants-2015_08 |