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HRID517177

反应详情

EQUATION

反应方程式

HRID 517177 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)CC(=O)CC(=O)C1
HCID31358

5,5-Dimethyl-1,3-cyclohexanedione

C8H12O2

结构：CC1(C)CCC(Nc2cccc(C(F)(F)F)c2)=CC1=O
HCID86732296

未命名化合物

2 次

PRODUCTS

生成物

1
结构：CC1(C)CC(=O)C=C(Nc2cccc(C(F)(F)F)c2)C1
HCID614722

5,5-dimethyl-3-[3-(trifluoromethyl)anilino]cyclohex-2-en-1-one

C15H16F3NO

PROCEDURE

实验过程

The title compound is prepared in analogy to 6,6-dimethyl-3-(3-(trifluoromethyl)phenyl-amino)cyclohex-2-enone (intermediate 6), using 5,5-dimethylcyclohexane-1,3-dione (1.13 g, 8.04 mmol) as starting material. Yield: 1.73 g, ESI mass spectrum [M+H]+=284, Retention time HPLC: 1.18 min (Z005—001).

WORKUP

后处理

  1. custom1.18 min (Z005—001)