HRID517205
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The title compound is prepared in analogy to 4-(4-bromo-2-(methylsulfonyl)phenyl)-1-(3-(trifluoromethyl)phenyl)-3,4,7,8-tetrahydroquinazoline-2,5(1H,6H)-dione (intermediate 34), using 1-(3-(difluoromethyl)phenyl)urea (intermediate 35, 707 mg, 3.80 mmol) as starting material. Yield: 319 mg; ESI mass spectrum [(79Br)-M+H]+=525, [(81Br)-M+H]+=527, Retention time HPLC: 1.01 min (Z017_S04).
WORKUP
后处理
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