HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-5-fluorobenzotrifluoride → HCID 59145682, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-5-fluorobenzotrifluoride | HCID 2735913 | — |
| Reactant | HCID 58266265 | HCID 58266265 | — |
| Product | HCID 59145682 | HCID 59145682 | — |
Reaction Steps
The title compound is prepared in analogy to 1-(4-fluoro-3-(trifluoromethyl)phenyl)urea (intermediate 42), using 5-fluoro-3-(trifluoromethyl)aniline (1.00 g, 5.58 mmol) as starting material. Yield: 630 mg; ESI mass spectrum [M+H]+=223; Retention time HPLC: 0.91 min (Z018_S04).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09115093B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-cf596e6230224507b13ba39804ed924a |
| Source note | uspto-grants-2015_08 |