HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 90404447, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 90404477 | HCID 90404477 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 90404447 | HCID 90404447 | — |
Reaction Steps
(sodium 5-methyl-3-(2H-1,2,3-triazol-2-yl)picolinate). To a solution of the title compound of Step A (489 mg, 2.6 mmol) in EtOH (7 mL) was added 4 N NaOH (660 μL, 2.6 mmol). The mixture was heated at 100° C. for 24 h. The reaction mixture was concentrated in vacuo to a white solid which was used without further purification in subsequent steps.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09115117B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-70c26e18996746aabc99ed362c39ff8f |
| Source note | uspto-grants-2015_08 |