HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 90405511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 90405754 | HCID 90405754 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Sodium Carbonate | HCID 10340 | — |
| Product | HCID 90405511 | HCID 90405511 | 76.9% |
Reaction Steps
To the title compound of step A (813 mg) in DCM (6 mL) was added TFA (2 mL). After 1 h, the reaction was diluted with saturated Na2CO3 (aq) and extracted with DCM. The organic layers were dried (MgSO4) and concentrated to give the title compound (452 mg) that was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09115117B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-7c18ba282cad498db99a35157d6dc45c |
| Source note | uspto-grants-2015_08 |