HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanesulfonyl chloride → HCID 178477703, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanesulfonyl chloride | HCID 82408 | — |
| Reactant | HCID 178522618 | HCID 178522618 | — |
| Product | HCID 178461040 | HCID 178461040 | — |
| Product | HCID 178477703 | HCID 178477703 | 19% |
Reaction Steps
The title compound was prepared from (E)-N-(6-(2-(piperidin-1-yl)ethoxy)-1-(piperidin-4-yl)-1H-imidazo[4,5-c]pyridin-2(3H)-ylidene)benzamide and 2-propanesulphonyl chloride using a method analogous to the preparation of (E)-N-(1-(1-(ethylsulfonyl)piperidin-4-yl)-6-(2-(piperidin-1-yl)ethoxy)-1H-imidazo[4,5-c]pyridin-2(3H)-ylidene)benzamide (20 mg, 19.0% yield). MS m/z=555.2 [M+H]. Calc'd for C28H38N6O4S: 554.3
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09115127B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-0c06cf1511554eb3b84ac430ca26fcbc |
| Source note | uspto-grants-2015_08 |