HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178468177, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178468181 | HCID 178468181 | — |
| Product | HCID 178468177 | HCID 178468177 | 100.3% |
Reaction Steps
A suspension of tert-butyl cis-4-acetylcyclohexylcarbamate (1.8 g, 7.46 mmol) in HCl (4M in dioxane) (93 mL, 373 mmol) was stirred at RT for 16 hours. The resulting mixture was concentrated to dryness to afford 1-(cis-4-aminocyclohexyl)ethanone hydrochloride as a white solid (1.33 g, 100% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09115127B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-d8c7c13a92c34c979198df7f3107fd6e |
| Source note | uspto-grants-2015_08 |