反应详情

A suspension of tert-butyl cis-4-acetylcyclohexylcarbamate (1.8 g, 7.46 mmol) in HCl (4M in dioxane) (93 mL, 373 mmol) was stirred at RT for 16 hours. The resulting mixture was concentrated to dryness to afford 1-(cis-4-aminocyclohexyl)ethanone hydrochloride as a white solid (1.33 g, 100% yield).

1. concentrationThe resulting mixture was concentrated to dryness