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HRID51880

反应详情

EQUATION

反应方程式

HRID 51880 的结构方程式

REACTANTS

反应物

6
结构：BrCc1ccccc1
HCID7498

alpha-Bromotoluene

C7H7Br

结构：O=C(O)c1ccc(F)cc1
HCID9973

Benzoic acid, 4-fluoro-

C7H5FO2

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CN(C)C(On1nnc2cccnc21)=[N+](C)C.F[P-](F)(F)(F)(F)F
HCID9886157

Methanaminium, N-((dimethylamino)(3H-1,2,3-triazolo(4,5-b)pyridin-3-yloxy)methylene)-N-methyl-, hexafluorophosphate(1-) (1:1)

C10H15F6N6OP

结构：CCNc1ccc(OC)c2nc(N)sc12
HCID22737006

未命名化合物

PRODUCTS

生成物

1
结构：CCN(Cc1ccccc1)c1ccc(OC)c2nc(NC(=O)c3ccc(F)cc3)sc12
HCID22737001

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

From N7-ethyl-4-methoxy-benzothiazole-2,7-diamine with potassium carbonate and benzyl bromide in DMF, then treatment with 4-fluorobenzoic acid, HATU and N-ethyldiisopropylamine in THF. ES-MS m/e (%): 436 (M+H+, 100).