Trifluoroacetic acid → HCID 86727435, compound

Participants

Reaction Steps

A solution of 6-(azetidin-3-ylamino)-4-methyl-7-phenoxy-2,10-dihydro-9-oxa-1,2,4a-triaza-phenanthren-3-one (0.015 g, 0.031 mmol) in DCM (3 mL) and TFA (0.5 mL) was stirred for 2 h at ambient temperature. The solvent was removed in vacuo to give 6-(azetidin-3-ylamino)-4-methyl-7-phenoxy-2,10-dihydro-9-oxa-1,2,4a-triaza-phenanthren-3-one trifluoroacetic acid (0.009 mg, 58%) as a white solid. LC/MS (Table 1, Method 5) Rt=2.166 min; MS m/z: 380 [M+H]+

Provenance & Evidence