Piperidine → HCID 86666422, compound

HRID 519419Notes

Reaction equation

HRID 519419 reaction equation
[Cl:1]([O-:5])(=[O:4])(=[O:3])=[O:2].CS[C:8]1[N:9]([CH3:18])[C:10]2[CH:17]=[CH:16][CH:15]=[CH:14][C:11]=2[N+:12]=1[CH3:13].[NH:19]1[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1>O1CCOCC1>[Cl:1]([O-:5])(=[O:4])(=[O:3])=[O:2].[NH:19]1[CH2:24][CH2:23][CH2:22][CH2:21][CH:20]1[C:8]1[N:9]([CH3:18])[C:10]2[CH:17]=[CH:16][CH:15]=[CH:14][C:11]=2[N+:12]=1[CH3:13]

Participants

4

Reactant 2

HCID 8082PiperidineHCID 14222620HCID 14222620, compound

Product 1

HCID 86666422HCID 86666422, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

Heat 0.01 mol of 2-methylmercapto-1,3-dimethylbenzimidazolium perchlorate with 0.01 mol of piperidine for 4th at reflux in 250 ml of dioxane. Remove the solids by suction and recrystallise from ethanol.

Workup

  1. customRemove the solids by suction
  2. customrecrystallise from ethanol

Sources & evidence

ORD record
ord-90bec4b255494ef5b4f10f1a108fd875
Source dataset
uspto-grants-2015_08
Patent number
US09118019B2

Reaction notes

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