HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11118994, compound → HCID 15647195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11118994 | HCID 11118994 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15647195 | HCID 15647195 | — |
Reaction Steps
A stirred suspension of diethyl 5-oxo-3,3a,4,5-tetrahydropentalene-2,2(1H)-dicarboxylate (322 mg, 1.209 mmol) and 10% Pd—C (129 mg, 0.121 mmol) in EtOH (40 mL) was hydrogenated under balloon pressure overnight. The suspension was filtered and the filtrate was evaporated to dryness to afford diethyl 5-oxohexahydropentalene-2,2(1H)-dicarboxylate as a clear oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09326973B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-2071b0e097c243a99b537e066820e0dc |
| Source note | uspto-grants-2016_05 |