HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethynyl-3-fluorobenzene → HCID 90031129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethynyl-3-fluorobenzene | HCID 520218 | — |
| Reactant | HCID 90031855 | HCID 90031855 | — |
| Product | HCID 90031129 | HCID 90031129 | 96% |
Reaction Steps
The title compound was prepared in accordance with the general method of Example 1, step 7 using (3aR,6aR)-1-(5-iodopyridin-2-yl)hexahydro-cyclopenta[b]pyrrol-2(1H)-one (107 mg, 0.326 mmol) (Example 1, step 6) and 1-ethynyl-3-fluorobenzene to yield 100 mg (96%) of the title compound as a viscous yellow oil; MS: m/e=321.2 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328090B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-ee7bb520f7d3424b82d3c59c40d865c8 |
| Source note | uspto-grants-2016_05 |