HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-(methylthio)aniline → N-[5-chloro-2-(methylthio)phenyl]-5-methylfuran-2-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-(methylthio)aniline | HCID 2794577 | — |
| Reactant | 5-Methylfuran-2-sulfonyl chloride | HCID 17864361 | — |
| Product | N-[5-chloro-2-(methylthio)phenyl]-5-methylfuran-2-sulfonamide | HCID 57378991 | 61.2% |
Reaction Steps
Following General Procedure B, the title compound (212 mg, 48%) was prepared from 5-chloro-2-methylsulfanyl-phenylamine (189 mg, 1.09 mmol) and 5-methyl-furan-2-sulfonyl chloride (250 mg, 1.38 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328067B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-37e3329a8466493ea98d31883409dba5 |
| Source note | uspto-grants-2016_05 |