HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl mercaptan → HCID 86690991, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl mercaptan | HCID 7509 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 6-bromo-5-nitro-2,3-dihydro-1H-inden-1-one | HCID 10060940 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86690991 | HCID 86690991 | 79% |
Reaction Steps
Following General Procedure A, the title compound (672 mg, 79%) was prepared from 6-bromo-5-nitro-2,3-dihydro-1H-inden-1-one (1.5 g, 5.86 mmol), phenylmethanethiol (1 ml, 8.79 mmol) and K2CO3 (4.0 g, 29.29 mmol) in DMF (20 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328067B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-7e8793c98df043eb9cb889aeea777781 |
| Source note | uspto-grants-2016_05 |