HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86729359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | tert-Butyl 4-(cyanomethylidene)piperidine-1-carboxylate | HCID 15326949 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86729359 | HCID 86729359 | — |
Reaction Steps
tert-Butyl 4-(cyanomethylidene)piperidine-1-carboxylate (20 g, 90 mmol) was dissolved in 4M HCl in dioxane and allowed to stir at ambient temperature for 2 hours. The mixture was then concentrated in vacuo to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328099B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-b70ba726cde840b3a1922d722ff86ca2 |
| Source note | uspto-grants-2016_05 |