Potassium Carbonate → HCID 11311797, compound

HRID 521518Notes

Reaction equation

HRID 521518 reaction equation
[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([O:19]C(=O)C)[CH:6]=1)[CH3:2].C(=O)([O-])[O-].[K+].[K+]>CO>[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([OH:19])[CH:6]=1)[CH3:2]

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 67170201HCID 67170201, compound

Product 1

HCID 11311797HCID 11311797, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of step 1 (10 g, 31.8 mmol) was dissolved in methanol, potassium carbonate (88 mg, 0.636 mmol) was added and the mixture was stirred for 2 h under reflux. After evaporation to dryness, the residue was used without further purification in the subsequent step.

Workup

  1. temperatureunder reflux
  2. customAfter evaporation to dryness
  3. customthe residue was used without further purification in the subsequent step

Sources & evidence

ORD record
ord-dfacff06dd0949c28dda9c235b25f569
Source dataset
uspto-grants-2016_05
Patent number
US09328071B2

Reaction notes

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